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Qualitative & Quantitative Analyzer

HPLC+GC-MS Triple analyzer, GC-MS, LC-MS, IC, FTIR, XRD, UV/Vis Spectrometer

XRD-2700 Series XRD Multi-functional X-ray Diffractometer

XRD-2700 시리즈 X-선 회절 분석기는 재료 연구 및 산업 제품 분석을 위해 설계되었으며 종래의 분석 기술과 특수 목적 측정 기법을 결합한 완벽한 제품입니다.

 

  • The perfect combining with hardware and software system, satisfy with the requirement of different application field academician, scientific research.
  • High precision diffraction angle measuring system, obtaining more accurate measurement results.
  • High stability X-ray generator control system, and get more stable repeatable measurement precision.
  • Various functional accessories meet the requirement of different testing purposes.
  • Program operation, integrated structure design, easy to operate, more beautiful appearance of the instrument;
  • X-ray diffractometer is a kind of universal testing instrument for revealing crystal structure and chemical information of material:
  • One and many phase identification of unknown sample
  • Quantitative analysis of the phase in the mixed sample
  • Crystal structure analysis (Rietveld structure analysis)
  • The crystal structure change (high temperature and low temperature condition) of the abnormal condition.
  • Thin film sample analysis, including film, multilayer film thickness, surface roughness, charge density.
  • Analysis of micro area sample.
  • Texture and stress analysis of metallic materials

 


 

Application


본 제품은 금속 재료 및 유.무기 재료, 복합 재료, 나노 소자, 초전도 소재에 적용 할 수 있습니다. 이들 재료 상태는 분말 또는 블록, 박막 및 마이크로 영역의 마이크로 샘플 일  수 있습니다.  본 제품은 점토 광물, 시멘트 건축 자재, 환경 먼지, 화학 제품, 약물, 석면, 암석, 폴리머 및 다양한 연구 분야에서 널리 사용됩니다.

 

Functions

  • Indicate the material’s crystal structure and chemical information;
  • Identify one or multiple phases in an unknown sample;
  • Quantitative analysis of the known phase in the mixed sample;
  • Crystallographic structural analysis (Rietveld structure analysis);
  • Measure the changes of crystal structure under normal conditions (low or high temperature);
  • Film sample analysis, including thin film phase, multi-films thickness, surface roughness and electric density;
  • Micro-area sample analysis;
  • Microstructure and stress analysis on metal material.Optional Multi-sample holder


 

Advantages

  • Base on θ-θ optical design it is easy for sample preparation and accessories installation;
  • Adopting metal ceramic X-ray tube improves the operating power of the XRD greatly;
  • Closed proportional counter is durable and maintenance free;
  • Silicon Drift Detector has superior angular resolution and energy resolution, the measuring speed can improve more than 3 times;
  • Various accessories can meet different analysis aims; Various function accessories automatic identification;
  • Base on modular design (plug and play configuration), operator can correctly use XRD without adjusting optical system.

 

Function of Software

  • Basic data processing (peak seeking, smoothing, background deduction, peak fitting, peak amplification, spectra comparison, Kα1 and α2K stripping, diffractive line indexing, etc.)
  • Quick quantitative analysis for samples without and reference parameters;
  • Size measurement of crystal grain;
  • Crystal structure analysis (parameter measurement and refining of unit cell);
  • Macroscopic stress measurement and micro stress calculation; 2d and 3d display of multiple drawings;
  • Diffraction peak image cluster analysis;
  • Diffraction data half-peak width correction curve;
  • Diffraction data Angle deviation correction curve;
  • General quantitative analysis Based on Rietveld;

 

Multi-function sample holder

With the deepening of material analysis, we want to do performance analysis by XRD on more materials, such as slabs, bulk material and film on matrix. Installing a multi-function sample holder on the goniometer can realize texture, macro-stress and film inner structure measurements. Each function has its own calculating software.


➢Texture measurement and evaluation on rolling plate (AL, Fe, Copper plate, etc)
➢Residual stress measurement on metal, ceramic, etc
➢Crystal preferred orientation evaluation on film sample
➢Orientation measurement on macromolecular compound
➢Multilayer film, oxidation film and nitride film analysis on the metals and non-metallic substrate

 

Multi-function sample holder is used for structure measurement, after calculation, it will draw out pole figure, inverse pole figure and ODF figure. Multi-function sample holder is used for macroscopic stress measurement. Set several Psi angles between -30-90° to make the sample tilt corresponding angles. At different Psi angles, it can measure angle deviation of specific crystal plane respectively and figure out the macro-stress of the sample.


 

 

Specification

 

XRD-2700A

XRD-2700B

Rated power

3kW (HF, HV control technology)

4kW

Tube voltage

10~60kV

Tube current

5~50mA

5~80mA

X-ray tube

             Metal ceramic tubeTarget material: Cu、Fe、Co、Cr、Mo, etc        

Power:2.4kW

Focus size

1×10mm or 0.4×14mm or 2×12mm

Stability

≤0.005%

≤0.01%

Goniometer structure

Sample level(θ~θ)

Radius of diffraction

225mm(or custom by request:150~285mm range)

2θ Scanning range

﹣6~160°(θs:﹣3~80°、θd:﹣3~80°)

Scanning speed

0.0012°~50°/min

Scanning fashion

θs/ θdlinkage /single acting; continuous, stepping and Omg

Minimal stepping angle

1/10000°

Angle repeatable accuracy

1/10000°

2θ Angular linearity

International standard sample(Si, Al203), the angle of all peak in full spectrum are not more than ±0.02°

Detector

Proportional counters(PC) or scintillation counter(SC), Silicon drift detector(SDD), High speed one-dimensional semiconductor array

detector

 Maximal countingrate of

linearity  

5×10CPS(PC、SC with the compensate function of miss counting)、15×10CPS (SDD)、

9×10CPS(one-dimensional array)

Energy resolution ratio

≤25% (PC、one-dimensional array)、≤50%(SC)、≤200eV(SDD)

Counting fashion

differential coefficient or integral, PHA automatically, dead time regulate

Stability of system measure

                                                  ≤0.01%

Scattered rays dose

≤1μSv/h(without X-ray protective device)

Instrument integrative stability

≤0.1%

≤0.5%

Dimension

1000 × 800 × 1600mm

XRD-2700 Series XRD Multi-functional X-ray Diffractometer 

 

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