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내화물 측정분석 솔루션

XRD (X-Ray Diffraction)

Ultra-fine Particle Size Analyzer

전자 현미경 (SEM+EDS)

만능재료시험기 (UTM)

압축 강도 시험기 (Hot modulus of rupture)

열간 곡강도 시험기 (Bending strength)

열간 선팽창 시험기 (TMA, Dilatometer)

열전도도측정기 (Thermal conductivity meter)

TGA (열중량분석기)

DSC (시차주사열량계)

XRF (X-Ray Fluorescence Spectrometer for RoHS)

X-ray fluorescence energy dispersive general purpose spectrometer BRA-135F

  • Essential auxiliary materials used as lining for ferrous and non-ferrous metals and alloys furnaces are refractories.

  • For Refractories and High-Temperature Ceramics

Refractories are rocks, minerals and their mixtures with the fusion temperature of over 1500ОС that do not interact with molten metals. Detectable elements in various types of refractories are Mg, Na, Al, Si, K, Ca, Ti, Cr, Fe, Zr. Requirements to methods for detection of these elements in these refractories are described in the standard [GOST 2642.0-86. Refractories and refractory raw material. General requirements to analysis methods.]. All these elements may be determined with spectrometer BRA-135 according to the procedure similar to procedure of rock silicate analysis method.

Currently the Russian Federation standard for X-ray fluorescence of refractory materials and high-temperature ceramics GOST R “Refractories. X-ray fluorescence analysis", which is a translation of the international standard [ISO 12677:2003 Chemical analysis of refractory products by X-ray fluorescence (XRF) – Fused cast bead method] is being developed. The goal of Russian Federation’s national standard development is direct application of international standard ISO 12677, with due regard of specific features of refractories X-ray fluorescence analysis in the Russian Federation. The standard allows for detecting contents of Na2O, MgO, Al2O3, SiO2, P2O5, SO3, K2O, CaO, TiO2, Cr2O3, Mn3O4, Fe2O3, Co3O4, NiO, ZrO2, WO3, BaO, SrO, HfO2, Y2O3, CeO2, La2O3, SnO2 within the range of 0.01% to 100%.

With specific features of Russian enterprises taken into account, this standard allows both the analysis of powder samples and sample preparation through fusion with lithium pyroborate, and concentration ranges of some elements have been changed. Analysis reproducibility and precision is better for fused samples, but analysis of compacted powder samples is allowed on most cases as well.